HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 73603937, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 73603938 | HCID 73603938 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 73603937 | HCID 73603937 | — |
Reaction Steps
2-[2-[(4aR,7aR)-2-amino-7a-pyrazin-2-yl-4,4a,5,7-tetrahydropyrrolo[3,4-d][1,3]thiazin-6-yl]-5-fluoro-pyrimidin-4-yl]propan-2-ol (120 mg, 0.308 mmol) is dissolved in 0.1 M HCl (3.1 mL) and acetonitrile (1 mL). The resulting solution is freeze dried to obtain the title compound as a white solid. ES/MS (m/e): 390 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09328124B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-1b851fd48198424db33a3927a15df3fb |
| Source note | uspto-grants-2016_05 |