HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → Trifluoroacetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 90409204 | HCID 90409204 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 90411970 | HCID 90411970 | — |
Reaction Steps
A mixture of Example 5C (8 g, 15.02 mmol) and trifluoroacetic acid (11.58 mL, 150 mmol) in dichloromethane (100 mL) was stirred at 20° C. for 12 hours and the mixture was concentrated to provide the title compound as a trifluoroacetic acid salt. MS (CI) m/z 432 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09328112B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-a01ba4491c5346c8b58912ca6b9899d3 |
| Source note | uspto-grants-2016_05 |