HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 118274116, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 118274223 | HCID 118274223 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 118274116 | HCID 118274116 | — |
Reaction Steps
A solution of Example 99C (1.135 g, 2.392 mmol) in dichloromethane (6 mL) was treated with trifluoroacetic acid (3 mL) at room temperature for 30 minutes, and concentrated in vacuo. The crude product (LC-MS 375.2 (M+H)+) was directly used for next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09328112B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-7c1edbee70894ebdac867a631e4eb192 |
| Source note | uspto-grants-2016_05 |