反应详情

To a stirred solution of 4-aminostyrene (3.5 mmol) in dry THF (20 mL) under nitrogen was added 3,5-bis-(trifluoromethyl)phenyl isothiocyanate (3.5 mmol). The solution was refluxed overnight and then the solvent was evaporated under reduced pressure. The resulting solid residue was purified by column chromatography to yield the desired product in 60% yield.

1. temperatureThe solution was refluxed overnight
2. customthe solvent was evaporated under reduced pressure
3. customThe resulting solid residue was purified by column chromatography