HRID522657

反应详情

EQUATION

反应方程式

HRID 522657 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a solution of tert-butyl 4-(5-(2-fluorophenoxyl)pyrimidin-2-yl)piperazine-1-carboxylate (50 mg, 0.13 mmol) in dioxane (3 mL) was added 4 M HCl/dioxane (3 mL). The reaction mixture was stirred at room temperature overnight and then concentrated to dryness. The residue (50 mg, yellow solid) was directly used in the next reaction.

WORKUP

后处理

  1. concentrationconcentrated to dryness
  2. customThe residue (50 mg, yellow solid) was directly used in the next reaction