HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 178524246, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 178497575 | HCID 178497575 | — |
| Reactant | HCID 178524247 | HCID 178524247 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178524246 | HCID 178524246 | — |
Reaction Steps
2-{4-[2-(3-Chloro-phenyl)-ethylamino]-2-oxo-1,2-dihydro-pyridin-3-yl}-3H-benzoimidazole-4-carboxylic acid was synthesized from 2-{4-[2-(3-chloro-phenyl)-ethylamino]-2-oxo-1,2-dihydro-pyridin-3-yl}-3H-benzoimidazole-4-carboxylic acid methyl ester, LiOH, THF, and water using a similar procedure as 2-[4-((S)-2-hydroxy-2-phenyl-ethylamino)-2-oxo-1,2-dihydro-pyridin-3-yl]-3H-benzoimidazole-4-carboxylic acid yielding 2-{4-[2-(3-chloro-phenyl)-ethylamino]-2-oxo-1,2-dihydro-pyridin-3-yl}-3H-benzoimidazole-4-carboxylic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09334480B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-1ce4f9d2d25746158f0cdc2cbff21a5d |
| Source note | uspto-grants-2016_05 |