Triethylamine → HCID 136268344, compound

Participants

Reaction Steps

2-Methylsulfanyl-5,6,7,8-tetrahydro-3H-quinazolin-4-one (100 mg; 0.51 mmol), N-(2-pyridyl)-2-(piperazin-1-yl)acetamide * 3HCl * 2H2O (279.5 mg; 0.76 mmol) and triethylamine (282.5 μl; 2.04 mmol) are reacted in isoamyl alcohol (2 ml) in accordance with the procedure for Example 9 (reaction time 8 h) and worked up. The crystals obtained are dissolved in acetonitrile and water and freeze-dried; yield: 19 mg (10%), crystals;

Provenance & Evidence