2-Methoxyethylamine → HCID 11473227, compound

HRID 523722Notes

Reaction equation

HRID 523722 reaction equation
C(O[C:6]([C:8]1[N:9]=[C:10]([Cl:23])[C:11]2[C:16]([C:17]=1[OH:18])=[CH:15][CH:14]=[C:13]([O:19][CH:20]([CH3:22])[CH3:21])[CH:12]=2)=[O:7])CCC.[CH3:24][O:25][CH2:26][CH2:27][NH2:28]>>[CH3:24][O:25][CH2:26][CH2:27][NH:28][C:6]([C:8]1[N:9]=[C:10]([Cl:23])[C:11]2[C:16]([C:17]=1[OH:18])=[CH:15][CH:14]=[C:13]([O:19][CH:20]([CH3:21])[CH3:22])[CH:12]=2)=[O:7]

Participants

3

Reactant 2

HCID 80182-MethoxyethylamineHCID 186981481-Chloro-4-hydroxy-7-isopropoxy-isoquinoline-3-carboxylic acid butyl ester

Product 1

HCID 11473227HCID 11473227, compound

Procedure

Synthesized from 1-chloro-4-hydroxy-7-isopropoxy-isoquinoline-3-carboxylic acid butyl ester (can be obtained according to U.S. Pat. No. 6,093,730, October 1998, Weidmann et al.) and 2-methoxy-ethylamine in analogy to example B-5; MS-(−)-ion: M−1=337.1.

Workup

  1. customcan be obtained

Sources & evidence

ORD record
ord-14eef3d4c4e64a678eca5e3aa3b64dae
Source dataset
uspto-grants-2016_05
Patent number
US09339527B2

Reaction notes

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