HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxy-3-(phenylmethoxy)benzeneacetonitrile → HCID 117396777, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxy-3-(phenylmethoxy)benzeneacetonitrile | HCID 117386008 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Ammonia | HCID 222 | — |
| Product | HCID 117396777 | HCID 117396777 | — |
Reaction Steps
7.7 g (34 mmol) (3-Benzyloxy-2-methoxy-phenyl)-acetonitrile (example XI) in 100 mL methanolic ammonia (c=7 mol/L) are hydrogenated (3 bar, r.t.) using 250 mg Raney-nickel. The reaction mixture is filtered and the solvent is removed in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09340510B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-025905235d474bd89d3d60bb448f96dd |
| Source note | uspto-grants-2016_05 |