Sulfuryl chloride → HCID 68781764, compound

Participants

Reaction Steps

5.0 g (31 mmol) 6-Methoxy-1,2,3,4-tetrahydro-isoquinoline in 30 mL AcOH are cooled to 0° C. and 2.7 mL (34 mmol) sulfuryl chloride are added slowly. The resulting mixture is stirred at r.t. over night. The solvent is removed in vacuo and the residue is treated with toluene/ACN 1:1. The precipitate is filtered off and dried at 40° C. in vacuo.

Provenance & Evidence