HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 118939106, compound → HCID 117998818, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 118939106 | HCID 118939106 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 117998818 | HCID 117998818 | — |
Reaction Steps
6.0 g (17 mmol) 6-Benzyloxy-4-hydroxy-3,4-dihydro-1H-isoquinoline-2-carboxylic acid tert-butyl ester (example XL) in 80 mL THF are hydrogenated (3 bar, r.t.) using 200 mg Pd/C (10%). The reaction mixture is filtered and the solvent is removed in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09340510B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-f1e4ae50eda14553a296d84c2d499f88 |
| Source note | uspto-grants-2016_05 |