Hydrochloric Acid → HCID 118939129, compound

Participants

Reaction Steps

To 200 mg (0.600 mmol) 6-cyclopropylmethoxy-4-methoxy-3,4-dihydro-1H-isoquinoline-2-carboxylic acid tert-butyl ester (example XLVI) in 3 mL dioxane are added 600 μL (2.40 mmol) HCl solution in dioxane (c=4 mol/L). After stirring over night at r.t. the reaction mixture is treated with DIPE, the precipitate is filtered off and dried at 40° C.

Provenance & Evidence