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HRID524353

反应详情

EQUATION

反应方程式

HRID 524353 的结构方程式

REACTANTS

反应物

2
结构：OB(O)c1cccc(C(F)F)c1
HCID44717244

[3-(Difluoromethyl)phenyl]boronic acid

C7H7BF2O2

结构：Cc1c(Br)c(=O)c(C(=O)NCc2ccc(S(C)(=O)=O)s2)cn1C(C)C
HCID89982807

未命名化合物

PRODUCTS

生成物

1
结构：Cc1c(-c2cccc(C(F)F)c2)c(=O)c(C(=O)NCc2ccc(S(C)(=O)=O)s2)cn1C(C)C
HCID89982809

未命名化合物

PROCEDURE

实验过程

Example 40 is prepared following the procedure for Example 24.1, substituting preparation 24 with preparation 39a and replacing 3-(trifluoromethyl)phenylboronic acid with 3-(difluoromethyl)phenylboronic acid. ESI mass spectrum: [M+H]+=495; Retention time HPLC: 0.82 min (Z011_S03).

WORKUP

后处理

  1. customExample 40 is prepared
  2. custompreparation 24