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HRID524355

反应详情

EQUATION

反应方程式

HRID 524355 的结构方程式

REACTANTS

反应物

2
结构：OB(O)c1cccc(C(F)F)c1
HCID44717244

[3-(Difluoromethyl)phenyl]boronic acid

C7H7BF2O2

结构：COC[C@@H](C)n1cc(C(=O)NCc2ccc(S(C)(=O)=O)cc2)c(=O)c(Br)c1C
HCID89978794

未命名化合物

PRODUCTS

生成物

1
结构：COC[C@@H](C)n1cc(C(=O)NCc2ccc(S(C)(=O)=O)cc2)c(=O)c(-c2cccc(C(F)F)c2)c1C
HCID89978697

未命名化合物

PROCEDURE

实验过程

Example 44 is prepared following the procedure for Example 24.1, substituting preparation 24 with preparation 43c and replacing 3-(trifluoromethyl)phenylboronic acid with 3-(difluoromethyl)phenylboronic acid. ESI mass spectrum: [M+H]+=519; Retention time HPLC: 0.97 min (Z018_S04).

WORKUP

后处理

  1. customExample 44 is prepared
  2. custompreparation 24
  3. custom0.97 min (Z018_S04)