反应详情

温度

60 °C

12.11 g (0.07 mol) of 2-furfurylthioacetamide was dissolved in 30 ml of pyridine. To the above solution, 9.94 g (0.07 mol) of benzoylchloride was added, and the mixture was stirred at 60° C. for 15 hours. The solvent was distilled away from the reaction mixture, and a residue thus obtained was added to ethyl acetate and washed successively with water twice, 1N hydrochloric acid, water three times, and brine. A resultant organic extract layer was dried, and the solvent was distilled away therefrom.

1. distillationThe solvent was distilled away from the reaction mixture
2. customa residue thus obtained
3. washwashed successively with water twice
4. customA resultant organic extract layer was dried
5. distillationthe solvent was distilled away