Hydrazine hydrate (1:1) → HCID 59322261, compound
Reaction equation
Cl[C:2]1[N:10]=[C:9]2[C:5]([N:6]=[CH:7][N:8]2[CH3:11])=[C:4]([NH:12][C:13]2[CH:20]=[CH:19][C:16]([C:17]#[N:18])=[CH:15][CH:14]=2)[N:3]=1.O.[NH2:22][NH2:23]>>[NH:22]([C:2]1[N:10]=[C:9]2[C:5]([N:6]=[CH:7][N:8]2[CH3:11])=[C:4]([NH:12][C:13]2[CH:20]=[CH:19][C:16]([C:17]#[N:18])=[CH:15][CH:14]=2)[N:3]=1)[NH2:23]Participants
3
Procedure
Was prepared according to Example 8 from 4-(2-chloro-9-methyl-9H-purin-6-ylamino)-benzonitrile and hydrazine monohydrate.
Workup
- customWas prepared
Sources & evidence
- ORD record
- ord-7206a70ccfc94801aee89ee23550d3f7
- Source dataset
- uspto-grants-2016_05
- Patent number
- US09340544B2
Reaction notes
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