Hydrazine hydrate (1:1) → (2-Hydrazino-9-methyl-9H-purin-6-yl)-phenethyl-amine

HRID 524530Notes

Reaction equation

HRID 524530 reaction equation
Cl[C:2]1[N:10]=[C:9]2[C:5]([N:6]=[CH:7][N:8]2[CH3:11])=[C:4]([NH:12][CH2:13][CH2:14][C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)[N:3]=1.O.[NH2:22][NH2:23]>>[NH:22]([C:2]1[N:10]=[C:9]2[C:5]([N:6]=[CH:7][N:8]2[CH3:11])=[C:4]([NH:12][CH2:13][CH2:14][C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)[N:3]=1)[NH2:23]

Participants

3

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 44324320(2-Chloro-9-methyl-9H-purin-6-yl)-phenethyl-amine

Product 1

HCID 59293639(2-Hydrazino-9-methyl-9H-purin-6-yl)-phenethyl-amine

Procedure

Was prepared according to Example 8 from (2-chloro-9-methyl-9H-purin-6-yl)phenethyl-amine and hydrazine monohydrate.

Workup

  1. customWas prepared

Sources & evidence

ORD record
ord-bb5953b455324d02a1730781a20365c1
Source dataset
uspto-grants-2016_05
Patent number
US09340544B2

Reaction notes

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