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HRID524617

反应详情

EQUATION

反应方程式

HRID 524617 的结构方程式

REACTANTS

反应物

1
结构：CC1(C)OCCN(Cc2ccccc2)[C@@H]1C(=O)OCc1ccccc1
HCID118118262

未命名化合物

PRODUCTS

生成物

1
结构：CC1(C)OCCN[C@@H]1C(=O)O
HCID90043546

未命名化合物

收率 70%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：[Pd]
催化剂HCID23938

Palladium

Pd

PROCEDURE

实验过程

(S)-benzyl 4-benzyl-2,2-dimethylmorpholine-3-carboxylate (10.4 g, 30.8 mmol) was reacted with H2 by Pd/C catalysis (10%, 1 g) according to the procedure as described in Example 34, Step C to give the title compound as a white solid (3.4 g, 70%). The compound was characterized by the following spectroscopic data: