HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 4-Methylpiperazine-2-carboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Ethyl 4-methylpiperazine-2-carboxylate | HCID 12558522 | — |
| Product | 4-Methylpiperazine-2-carboxylic acid | HCID 6420903 | 100% |
Reaction Steps
Ethyl 4-methylpiperazine-2-carboxylate (1.03 g, 6 mmol) was reacted with NaOH (0.48 g, 12 mmol) according to the procedure as described in Example 21, Step A to give the title compound as colorless oil (0.86 g, 100%). The compound was characterized by the following spectroscopic data:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09340538B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-88397e1baa204780b98e954df8ed3c75 |
| Source note | uspto-grants-2016_05 |