HCID 131735582, compound → HCID 84065206, compound

HRID 524792Notes

Reaction equation

HRID 524792 reaction equation
[CH3:1][O:2][C:3](=[O:22])[CH:4]=[CH:5][CH:6]1[O:11][CH2:10][CH2:9][N:8](C(OCC2C=CC=CC=2)=O)[CH2:7]1>[Pd]>[NH:8]1[CH2:9][CH2:10][O:11][CH:6]([CH2:5][CH2:4][C:3]([O:2][CH3:1])=[O:22])[CH2:7]1

Participants

3

Reactant 1

HCID 131735582HCID 131735582, compound

Product 1

HCID 84065206HCID 84065206, compoundYield 87.4%

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

Benzyl 2-(3-methoxy-3-oxoprop-1-en-1-yl)morpholine-4-carboxylate (6.47 g, 21.2 mmol) was reacted with Pd—C (10%, 0.65 g) according to the procedure as described in Example 34, Step C to give the title compound as colorless oil (3.21 g, 87%). The compound was characterized by the following spectroscopic data:

Sources & evidence

ORD record
ord-7468ba52c9a0409dbfb24af396ba7623
Source dataset
uspto-grants-2016_05
Patent number
US09340538B2

Reaction notes

Loading…