HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131735582, compound → HCID 84065206, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131735582 | HCID 131735582 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 84065206 | HCID 84065206 | 87.4% |
Reaction Steps
Benzyl 2-(3-methoxy-3-oxoprop-1-en-1-yl)morpholine-4-carboxylate (6.47 g, 21.2 mmol) was reacted with Pd—C (10%, 0.65 g) according to the procedure as described in Example 34, Step C to give the title compound as colorless oil (3.21 g, 87%). The compound was characterized by the following spectroscopic data:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09340538B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-7468ba52c9a0409dbfb24af396ba7623 |
| Source note | uspto-grants-2016_05 |