HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 20373768, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 84065206 | HCID 84065206 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20373768 | HCID 20373768 | 78% |
Reaction Steps
Methyl 3-(morpholin-2-yl)propanoate (0.58 g, 3.35 mmol) was reacted with a solution of NH3 in methanol (7 mol/L, 10 mL) according to the procedure as described in Example 25, Step A to give the title compound as brownish oil (0.41 g, 78%). The compound was characterized by the following spectroscopic data:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09340538B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-e592234e89e34abdb9f57c4fd94b7420 |
| Source note | uspto-grants-2016_05 |