HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Chloride → 6-Methoxybenzo[d]thiazole-2-carboximidamide hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | 2-Cyano-6-methoxy benzothiazole | HCID 342109 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Product | 6-Methoxybenzo[d]thiazole-2-carboximidamide hydrochloride | HCID 118107613 | 75% |
Reaction Steps
6-methoxybenzo[d]thiazole-2-carbonitrile (1 g, 5.26 mmol) was reacted with sodium methoxide (0.28 g, 5.26 mmol) and ammonium chloride (0.6 g, 11 mmol) according to the procedure as described in Example 61, Step B to give the title compound as a white solid (0.96 g, 75%). The compound was characterized by the following spectroscopic data:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09340538B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-a5da7ede6b604060ad6e1da9b0089605 |
| Source note | uspto-grants-2016_05 |