HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 118118263, compound → HCID 90042966, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 118118263 | HCID 118118263 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 90042966 | HCID 90042966 | 67% |
Reaction Steps
(S)-benzyl 4-benzyl-3-methylmorpholine-3-carboxylate (3.26 g, 10 mmol) was reacted with H2 by Pd/C catalysis (10%, 0.33 g) according to the procedure as described in Example 34, Step C to give the title compound as a gray solid (0.97 g, 67%). The compound was characterized by the following spectroscopic data:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09340538B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-58be9cf5a34143f3aed2d71a8f64f9bc |
| Source note | uspto-grants-2016_05 |