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HRID525682

反应详情

EQUATION

反应方程式

HRID 525682 的结构方程式

REACTANTS

反应物

2
结构：CNCCO
HCID8016

N-Methyl-N-hydroxyethylamine

C3H9NO

结构：O=C(Nc1ccc(SC(F)(F)F)cc1)c1cnc(Cl)c(Br)c1
HCID86702605

未命名化合物

PRODUCTS

生成物

1
结构：CN(CCO)c1ncc(C(=O)Nc2ccc(SC(F)(F)F)cc2)cc1Br
HCID89906571

未命名化合物

PROCEDURE

实验过程

The title compound was prepared in an analogous fashion to that described in Stage 22.1 using 5-bromo-6-chloro-N-(4-((trifluoromethyl)thio)phenyl)nicotinamide (Stage 25.2) and 2-methylamino-ethanol to afford an off-white crystalline solid. HPLC (Condition 4) tR=5.97 min, UPLC-MS (Condition 3) tR=1.18 min, m/z=450.2 [M+H]+.

WORKUP

后处理

  1. customto afford an off-white crystalline solid