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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 525682Generated: October 27, 2026

2-(Methylamino)ethanol → HCID 89906571, compound

https://huagongshe.com/reaction/525682

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-(Methylamino)ethanolHCID 8016—
Reactant5-bromo-6-chloro-N-(4-((trifluoromethyl)thio)phenyl)nicotinamideHCID 86702605—
ProductHCID 89906571HCID 89906571—

Reaction Steps

The title compound was prepared in an analogous fashion to that described in Stage 22.1 using 5-bromo-6-chloro-N-(4-((trifluoromethyl)thio)phenyl)nicotinamide (Stage 25.2) and 2-methylamino-ethanol to afford an off-white crystalline solid. HPLC (Condition 4) tR=5.97 min, UPLC-MS (Condition 3) tR=1.18 min, m/z=450.2 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09340537B2
Source datasetuspto-grants-2016_05
ORD IDord-8b316927dc414cb08ad69c1bc7abb814
Source noteuspto-grants-2016_05