HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4,6-Dichloro-1,5-naphthyridin-3-yl)ethan-1-one → HCID 178467144, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4,6-Dichloro-1,5-naphthyridin-3-yl)ethan-1-one | HCID 89704977 | — |
| Reactant | HCID 178483673 | HCID 178483673 | — |
| Product | HCID 178467144 | HCID 178467144 | 55.4% |
Reaction Steps
Following general procedure I, 1-(4,6-dichloro-1,5-naphthyridin-3-yl)ethanone (500 mg, 2.1 mmol) was reacted with cis-4-[(dimethylamino)methyl]cyclohexanamine (300 mg, 2.0 mmol) to afford the desired product (400 mg, 55%) as a yellow solid: ESI MS m/z 361 [M+H]+;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09345709B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-847fef2664794575927a90db8a6632a8 |
| Source note | uspto-grants-2016_05 |