HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylcarbodiimide → Chromocarb
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylcarbodiimide | HCID 12734 | — |
| Reactant | 4-Ethoxy-4-oxobutanoate | HCID 1711967 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Chromocarb | HCID 2741 | — |
Reaction Steps
LP-1 ctrl was synthesized by following Scheme 1 (FIG. 14). Rink SS resin was deprotected and loaded with monoethyl succinate (5 eq) and DIC (5 eq) in DMF for 2 hrs. The rest of the amino acids were added successively and the final product was purified by following the same methods described above.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09345789B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-c0ecd8d124ff4046b2cd3c322a7eedb2 |
| Source note | uspto-grants-2016_05 |