HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 86706428, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 15076055 | HCID 15076055 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86706428 | HCID 86706428 | — |
Reaction Steps
A solution of 2-isobutoxycarbonylamino-3-phenyl-propionic acid (5 gm), dichloromethane (25 mL) and dimethylformamide (0.5 mL) was cooled to 0-5° C. To the resulting solution, thionyl chloride (1.5 mL) was added at same temperature. The solvent was distilled out completely to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09346760B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-9590761eab8c45b3bcd017e3d9d663fb |
| Source note | uspto-grants-2016_05 |