HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 526735Generated: October 30, 2026
Boron trifluoride etherate → HCID 71152494, compound
https://huagongshe.com/reaction/526735
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Boron trifluoride etherate | HCID 8000 | — |
| Reactant | HCID 71152056 | HCID 71152056 | — |
| Catalyst | Mercuric acetate | HCID 15337 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 71152494 | HCID 71152494 | — |
Reaction Steps
A mixture of ethyl benzyl(4-hydroxybut-2-ynyl)carbamate (0.05 g, 0.202 mmol), mercury(II) acetate (6.44 mg, 0.020 mmol) and boron trifluoride etherate (5.12 μl, 0.040 mmol) in Acetonitrile (0.5 ml) and Water (0.250 ml) stirred at 90° C. in wheaton vial for 30 min. By HPLC-MS the main peak corresponds to expected product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09346751B2 |
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| Source dataset | uspto-grants-2016_05 |
|---|
| ORD ID | ord-8d41dc2a3ddb457f90d1c3e4bf4b78bb |
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| Source note | uspto-grants-2016_05 |
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