HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67811106, compound → HCID 118290572, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67811106 | HCID 67811106 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 118290572 | HCID 118290572 | 102.5% |
Reaction Steps
10% palladium carbon (40 mg) was added to a solution of 2-(6-hydroxy-4-methylbenzofuran-3-yl)acetic acid (200 mg) in methanol (3 mL), and the mixture was stirred at room temperature for 24 hours under a hydrogen atmosphere. The insoluble matter was filtered off, and then, the obtained filtrate was concentrated under reduced pressure to obtain the title compound (207 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09346776B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-15e3b974d3904e3e9769050fc6b59c4f |
| Source note | uspto-grants-2016_05 |