HCID 71295412, compound → 2,4-Dihydro-4-[4-[4-(4-hydroxyphenyl)-1-piperazinyl]phenyl]-2-(2-methylpropyl)-3H-1,2,4-triazol-3-one

Participants

Role	Name	HCID	Charge
Reactant	HCID 71295412	HCID 71295412	—
Solvent	Hydrogen Bromide	HCID 260	—
Product	2,4-Dihydro-4-[4-[4-(4-hydroxyphenyl)-1-piperazinyl]phenyl]-2-(2-methylpropyl)-3H-1,2,4-triazol-3-one	HCID 15125564	91%

Reaction Steps

This compound was synthesized as a white amorphous solid from 4f (64.0 mg, 0.152 mmol) in 48% aqueous HBr (1.5 mL) in 91% yield by following general procedure 1.4: MALDI-MS: 394.2 (M+H+), 416.2 (M+Na+).

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US09346791B2
Source dataset	uspto-grants-2016_05
ORD ID	ord-b14debb5235d4567b9fcf0e25156f8d6
Source note	uspto-grants-2016_05