HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Isopropylthio)benzylamine → 2-(4-(N-cyano-S-isopropylsulfinimidoyl)benzyl)isoindoline-1,3-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Isopropylthio)benzylamine | HCID 60884319 | — |
| Reactant | 2-(4-(N-cyano-S-ethylsulfinimidoyl)benzyl)isoindoline-1,3-dione | HCID 86711615 | — |
| Product | 2-(4-(N-cyano-S-isopropylsulfinimidoyl)benzyl)isoindoline-1,3-dione | HCID 86711618 | — |
Reaction Steps
The title compound is prepared in analogy to preparation 13a, substituting 4-(ethylthio)-benzylamine with 4-(isopropylthio)benzylamine ESI mass spectrum: [M+H]+=352; r.t. HPLC: 0.50 min (X012_S01).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09346794B1 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-1d800c98c8f14ddaa155bb2a15465f78 |
| Source note | uspto-grants-2016_05 |