反应详情

温度

110 °C

Phenol (376 g, 4 mol), hexadecene (α-olefin) (449 g, 2 mol) and ion exchange resin (trade-mark: Dia-ion RCP-145HD) (34 g) were charged in a reactor and stirred at 110° C. for 2 hours. The ion exchange resin was filtered off and the excessive phenol and hexadecene were distilled off under reduced pressure. After distillation under reduced pressure, mono-hexadecylphenol was obtained. The yield was 510 g.

1. filtrationThe ion exchange resin was filtered off
2. distillationthe excessive phenol and hexadecene were distilled off under reduced pressure
3. distillationAfter distillation under reduced pressure