Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | 1-Hexadecene | HCID 12395 | — |
| Product | Phenol, 4-hexadecyl- | HCID 75768 | — |
Reaction Steps
Phenol (376 g, 4 mol), hexadecene (α-olefin) (449 g, 2 mol) and ion exchange resin (trade-mark: Dia-ion RCP-145HD) (34 g) were charged in a reactor and stirred at 110° C. for 2 hours. The ion exchange resin was filtered off and the excessive phenol and hexadecene were distilled off under reduced pressure. After distillation under reduced pressure, mono-hexadecylphenol was obtained. The yield was 510 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05244588 |
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| Source dataset | uspto-grants-1993_09 |
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| ORD ID | ord-0a96ee7305764e7999d6459c776096d9 |
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| Source note | uspto-grants-1993_09 |
|---|
