HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 527852Generated: October 31, 2026
m-Chloroperbenzoic acid → 2-Methyl-propane-2-sulfonic acid (2-bromo-ethyl)-amide
https://huagongshe.com/reaction/527852
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | 2-Methyl-propane-2-sulfinic acid (2-bromo-ethyl)-amide | HCID 86713731 | — |
| Product | 2-Methyl-propane-2-sulfonic acid (2-bromo-ethyl)-amide | HCID 63688805 | 46.8% |
Reaction Steps
To a solution of 2-methyl-propane-2-sulfinic acid (2-bromo-ethyl)-amide (0.8 g, 3.5 mmol) was added mCPBA (77%, 0.95 g, 4.2 mmol) and stirred at a temperature of about 25° C. for 2 hrs. The reaction mixture was condensed and purified to provide 2-methyl-propane-2-sulfonic acid (2-bromo-ethyl)-amide as a white solid (0.4 g, 46% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09346808B2 |
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| Source dataset | uspto-grants-2016_05 |
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| ORD ID | ord-9955dfe097094ee2be6631161f9d01e9 |
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| Source note | uspto-grants-2016_05 |
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