Allylamine → HCID 39871266, compound

Participants

Reaction Steps

Allylamine (1.0 g, 17.5 mmol) was dissolved in dichloromethane (30 ml), 1,1′-carbonyldiimidazole (7.37 g, 15 mmol) was added, and the mixture was stirred overnight. The solvent was evaporated under reduced pressure, and the residue was partitioned between ethyl acetate and 1N hydrochloric acid. The organic layer was washed with saturated brine, and dried over anhydrous sodium sulfate, and the solvent was evaporated under reduced pressure to give the title compound.

Provenance & Evidence