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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 529227Generated: October 31, 2026

HCID 86714714, compound → HCID 68320279, compound

https://huagongshe.com/reaction/529227

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86714714HCID 86714714—
CatalystPalladium hydroxideHCID 9942167—
SolventMethanolHCID 887—
SolventChloroformHCID 6212—
ProductHCID 68320279HCID 68320279—

Reaction Steps

The compound (0.5 g, 1.45 mmol) obtained in step 1 was dissolved in methanol (5 mL) and chloroform (0.5 mL), palladium hydroxide (0.1 g) was added, and the mixture was dried at room temperature under a hydrogen atmosphere overnight. The reaction mixture was filtered through celite, and the solvent was evaporated under reduced pressure to give the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09346821B2
Source datasetuspto-grants-2016_05
ORD IDord-8509b9e8d46841a09c8dd7d44d88bfae
Source noteuspto-grants-2016_05