HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → HCID 118201132, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | Cyclobutylacetaldehyde | HCID 22386168 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 118201132 | HCID 118201132 | 105.8% |
Reaction Steps
Benzylamine (2.95 g, 27.5 mmol) was added to a mixture of cyclobutylacetaldehyde (30.6 mmol) in CH2Cl2 (˜238 mL) and molecular sieves (5.0 g) and the mixture was stirred at room temperature for 5.5 hours. The mixture was filtered over Celite and the solvent was removed under vacuum to yield 5.45 g of crude N-(2-cyclobutylethylidene)-1-phenylmethanamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09346853B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-68fd615743254ce5821775dd2ee41d1b |
| Source note | uspto-grants-2016_05 |