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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 529291Generated: October 30, 2026

Benzylamine → HCID 118201132, compound

https://huagongshe.com/reaction/529291

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzylamineHCID 7504—
ReactantCyclobutylacetaldehydeHCID 22386168—
SolventDichloromethaneHCID 6344—
ProductHCID 118201132HCID 118201132105.8%

Reaction Steps

Benzylamine (2.95 g, 27.5 mmol) was added to a mixture of cyclobutylacetaldehyde (30.6 mmol) in CH2Cl2 (˜238 mL) and molecular sieves (5.0 g) and the mixture was stirred at room temperature for 5.5 hours. The mixture was filtered over Celite and the solvent was removed under vacuum to yield 5.45 g of crude N-(2-cyclobutylethylidene)-1-phenylmethanamine.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09346853B2
Source datasetuspto-grants-2016_05
ORD IDord-68fd615743254ce5821775dd2ee41d1b
Source noteuspto-grants-2016_05