Isobutyric Acid → HCID 21900164, compound

HRID 530219Notes

Reaction equation

HRID 530219 reaction equation
[OH-].[CH2:2]([N+:6]([CH2:15][CH2:16][CH2:17][CH3:18])([CH2:11][CH2:12][CH2:13][CH3:14])[CH2:7][CH2:8][CH2:9][CH3:10])[CH2:3][CH2:4][CH3:5].[C:19]([OH:24])(=[O:23])[CH:20]([CH3:22])[CH3:21]>O>[C:19]([O-:24])(=[O:23])[CH:20]([CH3:22])[CH3:21].[CH2:15]([N+:6]([CH2:2][CH2:3][CH2:4][CH3:5])([CH2:7][CH2:8][CH2:9][CH3:10])[CH2:11][CH2:12][CH2:13][CH3:14])[CH2:16][CH2:17][CH3:18]

Participants

4

Reactant 2

HCID 6590Isobutyric AcidHCID 2723671Tetrabutylammonium Hydroxide

Product 1

HCID 21900164HCID 21900164, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

A 40 wt % solution of tetrabutylammonium hydroxide in water (250 mL, 99 g, 382 mmol), water (300 mL) and isobutyric acid (33.8 g, 382 mmol) was stirred at ambient temperature for 30 min. The solvent was removed in vacuo to afford the title compound (5) as a waxy solid, which was used without further purification.

Workup

  1. customThe solvent was removed in vacuo

Sources & evidence

ORD record
ord-f941a67dc7404d3d9c54c6879360f18b
Source dataset
uspto-grants-2016_05
Patent number
US09353057B2

Reaction notes

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