HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 178440148, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 2-propyl-1H-imidazole-4,5-dicarbonitrile | HCID 2763721 | — |
| Reactant | HCID 178461735 | HCID 178461735 | — |
| Product | HCID 178440148 | HCID 178440148 | — |
Reaction Steps
Following a procedure similar to that described in Preparation 23(i), but using 8.24 g of 2-propylimidazole-4,5-dicarbonitrile (prepared as described in Preparation 10) and 103 ml of a 2M solution of isopropylmagnesium iodide in diethyl ether, 45.0 g of the title compound were obtained as crystals, melting at 90.5°-91° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05616599 |
| Source dataset | uspto-grants-1997_04 |
| ORD ID | ord-32940677fdca4e678ac8efc29a977a23 |
| Source note | uspto-grants-1997_04 |