HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 530757Generated: November 3, 2026
Einecs 211-027-4 → HCID 178431895, compound
https://huagongshe.com/reaction/530757
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Einecs 211-027-4 | HCID 69401 | — |
| Reactant | 4-Methoxy-2-(4-methyl-thiazol-2-yl)-6-(4-trifluoromethyl-thiazol-2-yl)-pyridine | HCID 68159997 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178431895 | HCID 178431895 | 72% |
Reaction Steps
A mixture of compound 22 (1.68 mmol) and pyridinium chloride (5 g/mmol) was heated at 200° C. with stirring. After 30 min, the reaction mixture was cooled down to room temperature and H2O was added. The solid was collected, washed with H2O, and dried to give compound 23 as a grey solid in 72% yield. MS (ESI, EI+): m/z=343.85 (MH+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09353100B2 |
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| Source dataset | uspto-grants-2016_05 |
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| ORD ID | ord-079761f1ada8495e84cf02a2d56ba7ad |
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| Source note | uspto-grants-2016_05 |
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