HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azane;hydrate → (3-Ethyl-1-methyl-1H-pyrazol-5-yl)methanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azane;hydrate | HCID 12896473 | — |
| Reactant | 5-(bromomethyl)-3-ethyl-1-methyl-1H-pyrazole | HCID 66120941 | — |
| Product | (3-Ethyl-1-methyl-1H-pyrazol-5-yl)methanamine | HCID 23006075 | — |
Reaction Steps
A solution of compound 5 (660 mg, 3.27 mmol) in NH3.H2O (5 mL) was stirred at 90° C. for 3 h. The solvent was evaporated to give the crude product as a white solid which was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09353104B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-0c8ed6d935c14741b775cb62fa8cff82 |
| Source note | uspto-grants-2016_05 |