Hydrochloric Acid → HCID 54338057, compound

HRID 531409Notes

Reaction equation

HRID 531409 reaction equation
[C:1]1([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][Si:25]([O:32][CH2:33]C)([O:29][CH2:30]C)[O:26][CH2:27]C)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Cl>CO>[C:1]1([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][Si:25]([O:32][CH3:33])([O:26][CH3:27])[O:29][CH3:30])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 131735660HCID 131735660, compound

Product 1

HCID 54338057HCID 54338057, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The 18-phenyl octadecyl triethoxysilane obtained was subjected to alcohol exchange reaction in methanol having a small quantity of hydrochloric acid dissolved therein to obtain 6.5 g of 18-phenyl octadecyl trimethoxysilane. The purity by HPLC was 89.4%.

Workup

  1. dissolutiondissolved

Sources & evidence

ORD record
ord-944ad4896bd14f03a444f001a1022c7d
Source dataset
uspto-grants-2016_05
Patent number
US09353288B2

Reaction notes

Loading…