Caprolactam → HCID 131735662, compound

HRID 531426Notes

Reaction equation

[Cl-].[Cl-].[Zn+2:3].[OH-].[Na+].[C:6]1(=[O:13])[NH:12][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7]1>>[O-2:13].[Zn+2:3].[C:6]1(=[O:13])[NH:12][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7]1

Participants

Reactant 3

HCID 7768Caprolactam2×

HCID 14798Sodium Hydroxide

HCID 3007855Zincchloride2×

Product 1

HCID 131735662HCID 131735662, compound

Conditions

Temperature: 100 °C

Procedure

3.4 g ZnCl2 and 100 g caprolactam having a purity not less than 60% and a moisture not more than 20% are added to a reactor, and then stirred for 30 min at the temperature of 80° C., so that ZnCl2 is fully dissolved in a molten caprolactam solvent. 2 g NaOH is rapidly added under stirring for the purpose of reaction at 100° C. for 2 h to obtain nano zinc oxide/caprolactam mixture.

Sources & evidence

ORD record: ord-2ec34732c6f6445aa63b899d07328ba1
Source dataset: uspto-grants-2016_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09355765B2

Reaction notes

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