Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Caprolactam | HCID 7768 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Zincchloride | HCID 3007855 | — |
| Product | HCID 131735662 | HCID 131735662 | — |
Reaction Steps
3.4 g ZnCl2 and 100 g caprolactam having a purity not less than 60% and a moisture not more than 20% are added to a reactor, and then stirred for 30 min at the temperature of 80° C., so that ZnCl2 is fully dissolved in a molten caprolactam solvent. 2 g NaOH is rapidly added under stirring for the purpose of reaction at 100° C. for 2 h to obtain nano zinc oxide/caprolactam mixture.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09355765B2 |
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| Source dataset | uspto-grants-2016_05 |
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| ORD ID | ord-2ec34732c6f6445aa63b899d07328ba1 |
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| Source note | uspto-grants-2016_05 |
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