Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Caprolactam | HCID 7768 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Palladium Chloride | HCID 24290 | — |
| Product | HCID 86710476 | HCID 86710476 | — |
Reaction Steps
5.0 g PdCl2 and 100 g molten caprolactam having a purity not less than 80% and a moisture not more than 20% are added to a reactor, and then stirred for 30 min at the temperature of 100° C., so that PdCl2 is fully dissolved in a molten caprolactam solvent. 1 g NaOH is rapidly added under stirring for the purpose of reaction for 2 h at the temperature of 100° C., and then, 2 g KBH4 is added for continuous reaction for 2 h to obtain nano Pd/caprolactam mixture.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09355765B2 |
|---|
| Source dataset | uspto-grants-2016_05 |
|---|
| ORD ID | ord-cfad22c8bdd345e88282666a49c23a4e |
|---|
| Source note | uspto-grants-2016_05 |
|---|
