Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 531716Generated: October 30, 2026

HCID 118523895, compound → HCID 118523928, compound

https://huagongshe.com/reaction/531716

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 118523895HCID 118523895—
SolventTrifluoroacetic acid methylene chlorideHCID 21863450—
ProductHCID 118523928HCID 118523928205%

Reaction Steps

Using similar reaction conditions as described in step-ii of example-7, tert-butyl 4-(4-(3-(1-phenethyl-1H-pyrazol-4-yl)-1-tosyl-1H-pyrrolo[2,3-b]pyridin-5-yl)phenyl)piperazine-1-carboxylate (200 mg, 0.290 mmol) was deprotected in TFA/DCM (2/5 ml) to afford 175 mg (85.7% yield) of the titled compound. MS: m/z=589.2 (M+1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09353107B2
Source datasetuspto-grants-2016_05
ORD IDord-2ecf7bb3071c41049f649e5af5fb85d6
Source noteuspto-grants-2016_05