反应详情

To a solution of tert-butyl 2-(5-fluoro-2-nitrophenoxy)propylcarbamate (3.1 g) in MeOH (5 ml) was added 10% palladium on carbon (300 mg) and the reaction mixture was hydrogenated at room temperature at 50 psi. The catalyst was filtered off and the filtrate was concentrated in vacuo.

1. customwas hydrogenated at room temperature at 50 psi
2. filtrationThe catalyst was filtered off
3. concentrationthe filtrate was concentrated in vacuo