HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58413322, compound → HCID 58413335, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58413322 | HCID 58413322 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 58413335 | HCID 58413335 | — |
Reaction Steps
To a solution of Ethyl 3-(5-fluoro-2-nitrophenoxy)butanoate (1.3 g) in THF (50 ml) was added Raney nickel (150 mg) and the reaction mixture was hydrogenated. The catalyst was filtered off and the filtrate was concentrated in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08853193B2 |
| Source dataset | uspto-grants-2014_10 |
| ORD ID | ord-a28b34769c7d485f8ff2a6a776d9146c |
| Source note | uspto-grants-2014_10 |